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HomeAnnals of Tropical Researchvol. 48 no. 1 (2026)

Functional, Physicochemical, and Sensory Properties of Spray-Dried Encapsulated Cinnamon (Cinnamomum Mercadoi)

Jessabell Q. Cabada | Jan Isobel C. Hidalgo | Ruby E. Peralta | Kierby B. Depalan | Madelaine S. Dumandan | Genessa Jesy T. Pagote | Kervin B. Untalan

 

Abstract:

Background: Cinnamomum mercadoi is a Philippine native cinnamon species with promising bioactive properties. Despite extensive research on the majority of cinnamon varieties, studies regarding its potential as a functional food ingredient have not been fully established, particularly in terms of its techno-functional performance in food systems. Objective: This study aimed to develop and characterize microencapsulated C. mercadoi extract using maltodextrin and gum arabic materials, focusing on their functional, physicochemical, and sensory properties. Methods:Microencapsulation was performed via spray drying, employing different wall materials to stabilize the bioactive compounds. Total phenolic content (TPC) and antioxidant activity were determined to assess the retention of endogenous functional constituents. Physicochemical properties, including moisture content, water activity, solubility, bulk density, and wettability, were analyzed to assess storage stability and applicability in food matrices. Sensory acceptability was evaluated by a trained panel based on color, aroma, texture, taste, and general acceptability. Results: The optimized formulation achieved a TPC of 5.71mg GAE/g and strong antioxidant capacity (72.8% inhibition; 187.1 mmol TE/g), indicating effective preservation of bioactive compounds. Significant interactions among carrier ratios and drying temperature influenced moisture content, water activity, solubility, and bulk density. Moisture content ranged from 6.85% to 10.15%, while water activity values (0.40–0.66) suggested favorable storage stability. The powders exhibited good solubility and wettability, supporting compatibility with liquid food systems. Sensory evaluation showed no significant differences (p > 0.05) in color, aroma, taste, and overall acceptability, with mean hedonic scores corresponding to “like moderately.” Conclusion: The findings demonstrate the technological feasibility of producing stable, antioxidant-rich microencapsulated cinnamon extract suitable for functional foods and nutraceutical applications.



References:

  1. Bacon, R. F. (1909). Philippine terpenes and essential oils, III. The Philippine Journal of Science, 4(2), 114–115.
  2. Bakry, A. M., Abbas, S., Ali, B., Majeed, H., Abouelwafa, M. Y., Mousa, A., & Liang, L. (2016). Microencapsulation of oils: A comprehensive review of benefits, techniques, and applications. Comprehensive Reviews in Food Science and Food Safety, 15(1), 143–182.
  3. Bhandari, B. R., & Howes, T. (1997). Implication of glass transition for the drying and stability of dried foods. Journal of Food Engineering, 40(1–2), 71–79.
  4. Bhandari, B. R., & Howes, T. (2009). Implications of maltodextrin and drying conditions on the solubility of spray-dried powders. Food Research International, 42(1), 75–82
  5. Bradley, R. L. (2010). Moisture and total solids analysis. In S. S. Nielsen (Ed.), Food analysis (4th ed., pp. 85–104). .
  6. Cai, Y. Z., & Corke, H. (2000). Production and properties of spray-dried Amaranthus betacyanin pigments. Journal of Food Science, 65(7), 1248–1252.
  7. Caliskan, G., & Dirim, S. N. (2013). The effects of different drying conditions and the amounts of maltodextrin addition during spray drying of sumac extract. Food and Bioproducts Processing, 91(4), 539–548.
  8. Carneiro, H. C. F., Tonon, R. V., Grosso, C. R. F., & Hubinger, M. D. (2013). Encapsulation efficiency and oxidative stability of flaxseed oil microencapsulated by spray drying using different combinations of wall materials. Journal of Food Engineering, 115(4), 443–451.
  9. Castillo-Israel, K. A. T., Sartagoda, K. J. D., Ilano, M. C. R., Flandez, L. E. L., Compendio, M. C. M., & Morales, D. B. (2020). Antioxidant properties of Philippine bignay (Antidesma bunius (Linn.) Spreng cv. ‘Common’) flesh and seeds as affected by fruit maturity and heat treatment. Food Research, 4(6), 1980–1987.
  10. Couto, R. O., Conceição, E. C., Chaul, L. T., Oliveira, E. M. S., Martins, F. S., Bara, M. T. F., Rezende, K. R., Alves, S. F., & de Paula, J. R. (2011). Spray-dried rosemary extracts: Physicochemical and antioxidant properties. Food Chemistry, 131(1), 99–105.
  11. Damodaran, S., Parkin, K. L., & Fennema, O. R. (Eds.). (2007). Fennema’s food chemistry (4th ed.). .
  12. de Souza, V. R., Pereira, P. A. P., da Silva, T. L. T., de Oliveira Lima, L. C., Pio, R., & Queiroz, F. (2014). Determination of the bioactive compounds, antioxidant activity and chemical composition of Brazilian blackberry, red raspberry, strawberry, blueberry and sweet cherry fruits. Food Chemistry, 156, 362–368.
  13. Fadel, H. H. M., Attia, G. H., & El-Ghorab, A. H. (2019). Microencapsulation of cinnamon essential oil by spray drying and evaluation of its antioxidant and antimicrobial activities. Food Chemistry, 287, 82–89.
  14. Fazaeli, M., Emam-Djomeh, Z., Ashtari, A. K., & Omid, M. (2012). Effect of spray drying conditions and feed composition on the physical properties of black mulberry juice powder. Food and Bioproducts Processing, 90(4), 667–675.
  15. Felix, P. H. C., Birchal, V. S., Botrel, D. A., Marques, G. R., & Borges, S. V. (2017). Physicochemical and thermal stability of microcapsules of cinnamon essential oil by spray drying. Journal of Food Processing and Preservation, 41(3), Article e12919.
  16. Fennema, O. R. (1996). Food chemistry (3rd ed.).
  17. Forest Products Research and Development Institute. (2017). Philippine cinnamon: Important lesser-known forest resource.
  18. Gharsallaoui, A., Roudaut, G., Chambin, O., Voilley, A., & Saurel, R. (2007). Applications of spray-drying in microencapsulation of food ingredients: An overview. Food Research International, 40(9), 1107–1121.
  19. Hajimonfarednejad, M., Ostovar, M., Raee, M. J., Hashempur, M. H., Mayer, J. G., & Heydari, M. (2019). Cinnamon: A systematic review of adverse events. Clinical Nutrition, 38(2), 594–602.
  20. Hermanto, R. F., Khasanah, L. U., Kawiji, Atmaka, W., Manuhara, G. J., & Utami, R. (2016). Physical characteristics of cinnamon oil microcapsule. IOP Conference Series: Materials Science and Engineering, 107(1), 012064.
  21. Ho, T. M., Truong, T., & Bhandari, B. R. (2017). Methods to characterize the structure of food powders – A review. Bioscience, Biotechnology, and Biochemistry, 81(4), 651–671.
  22. Hu, Q., Li, X., Chen, F., Wan, R., Yu, C. W., Li, J., McClements, D. J., & Deng, Z. (2020). Microencapsulation of an essential oil (cinnamon oil) by spray drying: Effects of wall materials and storage conditions on microcapsule properties. Journal of Food Processing and Preservation, 44(11), e14805.
  23. Julianti, E., Rajah, K. K., & Fidrianny, I. (2017). Antibacterial activity of ethanolic extract of cinnamon bark, honey, and their combination effects against acne-causing bacteria. Scientia Pharmaceutica, 85(2), 19.
  24. Klinkesorn, U., Sophanodora, P., Chinachoti, P., Decker, E. A., & McClements, D. J. (2005). Stability of spray-dried tuna oil emulsions encapsulated with two-layered interfacial membranes. Journal of Agricultural and Food Chemistry, 53(21), 8365–8371.
  25. Labuza, T. P., & Altunakar, B. (2007). Water activity prediction and moisture sorption isotherms. In G. V. Barbosa-Cánovas, A. J. Fontana Jr., S. J. Schmidt, & T. P. Labuza (Eds.), Water activity in foods: Fundamentals and applications (pp. 109–154). Blackwell Publishing.
  26. Lawless, H. T., & Heymann, H. (2010). Sensory evaluation of food: Principles and practices (2nd ed.). Springer.
  27. Li, L., Chen, L., Pan, D., Zhu, Y., Huang, R., Chen, J., Ye, C., & Yao, S. (2024). Evaluation of different drying methods on the quality of Cinnamomum cassia barks by analytic hierarchy process method. Heliyon, 10, e34608.
  28. Nadali, N., Pahlevanlo, A., Sarabi-Jamab, M., & Balandari, A. (2021). Effect of maltodextrin with different dextrose equivalents on the physicochemical properties of spray-dried barberry juice (Berberis vulgaris L.). Journal of Food Science and Technology, 59(7), 2855–2866.
  29. Nascimento, A. P. S., De Souza, J. M., Medeiros, D. F., Silva, A. S., & Silva, R. B. (2023). Enhancing antioxidant retention through varied wall-material compositions: Effects of whey, pectin, and gum arabic on phenolic compound stability. Antioxidants, 12(9), 1745.
  30. Navarro-Flores, M. J., Ventura-Canseco, L. M. C., Meza-Gordillo, R., Ayora-Talavera, T. R., & Abud-Archila, M. (2020). Spray drying encapsulation of a native plant extract rich in phenolic compounds with combinations of maltodextrin and non-conventional wall materials. Journal of Food Science and Technology, 57(11), 4111–4122.
  31. Olatunde, O. O., & Benjakul, S. (2018). Natural preservatives for extending shelf-life of seafood: A review. Comprehensive Reviews in Food Science and Food Safety, 17(6), 1595–1612.
  32. Ostroschi, L. C., de Souza, V. B., Echalar-Barrientos, M. A., Tulini, F. L., Comunian, T. A., Thomazini, M., et al. (2018). Production of spray-dried proanthocyanidin-rich cinnamon (Cinnamomum zeylanicum) extract as a potential functional ingredient: Improvement of stability, sensory aspects and technological properties. Food Hydrocolloids, 79, 343–351.
  33. Pérez-Alonso, C., Cruz-Olivares, J., Barrera-Pichardo, J. F., Rodríguez-Huezo, M. E., Báez-González, J. G., & Vernon-Carter, E. J. (2008). DSC thermo-oxidative stability of red chili oleoresin microencapsulated in blended biopolymers matrices. Journal of Food Engineering, 85(4), 613–624.
  34. Pisoschi, A.-M., Cheregi, M. C., & Danet, A. F. (2009). Total antioxidant capacity of some commercial fruit juices: Electrochemical and spectrophotometrical approaches. Molecules, 14(1), 480–493.
  35. Ramos, R. E., Balagot, K. W. M., Delica-Balagot, K. M., Samiano, F. B., Collera, J. J. A., & Lapuz, R. B. (2025). Evaluation of phytochemical components and antimicrobial activities of Philippine cinnamon (Cinnamomum mercadoi S. Vidal) extracts and essential oils. Philippine Journal of Science, 154(S1), 125–136.
  36. Reineccius, G. A. (2004). The spray drying of food flavors. Drying Technology, 22(6), 1289–1324.
  37. Rocha, R. P., Melo, E. C., & Radünz, L. L. (2011). Influence of drying process on the quality of medicinal plants: A review. Journal of Medicinal Plants Research, 5(33), 7076–7084.
  38. Sarabandi, K., Peighambardoust, S. H., Sadeghi Mahoonak, A. R., & Samaei, S. P. (2018). Effect of different carriers on microstructure and physical characteristics of spray dried apple juice concentrate. Journal of Food Science and Technology, 55(8), 3098–3109.
  39. Sidlagatta, V., Chilukuri, S. V. V., Devana, B. R., Dasi, S. D., & Rangaswamy, L. (2020). Effect of maltodextrin concentration and inlet air temperature on properties of spray dried powder from reverse osmosis concentrated sweet orange juice. Brazilian Archives of Biology and Technology, 63, e20190538.
  40. Stone, H., & Sidel, J. L. (2004). Sensory evaluation practices (3rd ed.). Elsevier Academic Press.
  41. Tonon, R. V., Brabet, C., & Hubinger, M. D. (2008). Influence of process conditions on the physicochemical properties of açaí (Euterpe oleracea Mart.) powder produced by spray drying. Journal of Food Engineering, 88(3), 411–418.
  42. Tonon, R. V., Grosso, C. R. F., & Hubinger, M. D. (2010). Influence of emulsion composition and inlet air temperature on the microencapsulation of flaxseed oil by spray drying. Food Research International, 44(1), 282–289.
  43. Torres, R. C., Sison, F. M., & Ysrael, M. C. (2003). Phytochemical screening and biological studies on the crude methanol extract of Cinnamomum mercadoi Vidal. Philippine Journal of Science, 132(1), 27–32.
  44. Wijewardhana, U. S., Gunathilaka, U. G. S. A., & Navaratne, S. B. (2019). Determination of total phenolic content, radical scavenging activity and total antioxidant capacity of cinnamon bark, black cumin seeds and garlic. International Research Journal of Advanced Engineering and Science, 4(2), 55–57.
  45. Wong, Y. C., Ahmad-Mudzaqqir, M. Y., & Wan-Nurdiyana, W. A. (2014). Extraction of essential oil from cinnamon (Cinnamomum zeylanicum). Oriental journal of chemistry, 30(1), 37.